مشخصات پژوهش

صفحه نخست /Synthesis and ...
عنوان Synthesis and characterization of novel hercynite@sulfuric acid and its catalytic applications in the synthesis of polyhydroquinolines and 2,3-dihydroquinazolin- 4(1H)-ones
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها hercynite@sulfuric acid; 2,3-dihydroquinazolin-4(1H)-one; polyhydroquinolines; nanomagnetic solid acid
چکیده Herein, we report the synthesis of hercynite@sulfuric acid as a novel nanomagnetic solid acid catalyst, containing the sulfuric acid catalytic sites on the surface of hercynite MNPs as the catalytic support. The assynthesized nanocomposite was meticulously characterized using a wide range of physicochemical techniques; including, FT-IR, XRD, EDX, X-ray-mapping, SEM and VSM analysis. The catalytic activity of this nanomagnetic material was considered for the synthesis of the diversely substituted polyhydroquinolines and 2,3-dihydroquinazolin-4(1H)-ones under solvent free conditions and also cyclocondensation reactions in ethanol, respectively affording good to excellent yields. Moreover, it is worth mentioning that the heterogeneity of the catalyst was measured through its excellent reusability and hot-filtration test.
پژوهشگران مسعود محمدی (نفر اول)، آرش قربانی چقامارانی (نفر دوم)