مشخصات پژوهش

صفحه نخست /Design, preparation and ...
عنوان Design, preparation and application of the s emi car baz ide ‑py rid oyl ‑sulfonic acid‑based nanocatalyst for the synthesis of pyranopyrazoles
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها pyranopyrazoles.s emi car baz ide ‑py rid oyl ‑sulfonic acid
چکیده A novel, efficient, and recoverable nanomagnetic catalyst bearing the semicarbazide linkers, namely, Fe3O4@ SiO2@OSi(CH2)3-N(3-pyridoyl sulfonic acid)semicarbazide (FSiPSS) was designed, synthesized and characterized by the use of various techniques such as FT‐IR, EDX, elemental mapping analysis, XRD, SEM, TEM, TGA/DTA, BET, and VSM. Then, the catalytic capability of the novel prepared nanomagnetic FSiPSS catalyst was successfully investigated in the synthesis of diverse pyranopyrazoles through a one-pot four-component condensation reaction of ethyl acetoacetate, hydrazine hydrate, aromatic aldehydes, and malononitrile or ethyl cyano-acetate by the help of ultrasonication in very short reaction time, good to high yields and easy work-up
پژوهشگران معصومه بیرانوند (نفر اول)، داود حبیبی (نفر دوم)