عنوان
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Application of 1‐methyl imidazole‐based ionic liquid‐stabilized silica‐coated Fe3O4 as a novel modified magnetic nanocatalyst for the synthesis of pyrano[2,3‐d]pyrimidines
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نوع پژوهش
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مقاله چاپشده در مجلات علمی
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کلیدواژهها
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aldehydes, barbituric acid, malononitrile, nanoparticles, pyrano[2,3-d] pyrimidines
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چکیده
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1-Methyl imidazole-based ionic liquid-stabilized silica-coated Fe3O4 magnetic nanoparticles [Fe3O4@SiO2@(CH2)3-1-methyl imidazole]HSO4 as a solid acid magnetic nanocatalyst was explored in the synthesis of pyrano[2,3-d]pyrimidine derivatives. Pyrano[2,3-d]pyrimidine derivatives were synthesized by a highly efficient three-component reaction of various benzaldehydes, malononitrile, and barbituric acid. The catalyst was characterized by using various analysis techniques such as Fourier transform infrared (FT-IR) spectroscopy, X-ray diffraction (XRD), differential scanning calorimetry-thermogravimetry analysis (DSC-TGA), scanning electron microscopy (SEM), and vibrating sample magnetometry (VSM).
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پژوهشگران
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سامی سجادی فر (نفر اول)، فرزانه تامی (نفر سوم)
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