مشخصات پژوهش

صفحه نخست /Synthesis of nano meta silica ...
عنوان Synthesis of nano meta silica sulfuric acid (NMSSA) as a novel heterogeneous catalyst for the preparation of dihydropyrimidinones under mild and green conditions
نوع پژوهش مقاله ارائه شده کنفرانسی
کلیدواژه‌ها dihydropyrimidinones
چکیده Heterogeneous catalysts have attracted considerable interest from both environmental and economical points. The solid acids have high turnover numbers (TON) and easily separated from reaction mixtures.1-2 Design, synthesis and applications of catalytic systems have more demand, because catalysis has played a major role in the preventing of pollution in our environment. Therefore , we wish to report synthesis of a novel nano-sized solid acid namely nono meta silica sulfuric acid (NMSSA) as a heterogeneous catalyst for the multicomponent synthesis such as 3,4-dihydropyrimidin-2(1H)-ones in excellent yields and short reaction time.3 NMSSA was synthesized from silicate anion and chlorosulfonic acid (Scheme 1). The described solid acid was characterized by XRD, FT-IR, TEM and SEM. We thought that the abovementioned nano solid acid is an alternative for heteropoly acids and have potential for industrial production.
پژوهشگران محمدعلی زلفی گل (نفر اول)، حسین قادری (نفر دوم)، لیلا محمدی (نفر سوم)