مشخصات پژوهش

صفحه نخست /Programming of ...
عنوان Programming of microwave-assisted synthesis of new isophthalatederivatives using ZrOCl2as a catalyst under solvent-free condition byexperimental design
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها MicrowaveDesign of experimentOptimizationIsophthalateZrOCl2
چکیده tIn this investigation, isophthalate derivatives were prepared by the reaction of isophthaloyl dichloridewith various alcohol derivatives using ZrOCl2as an efficient, green and a heterogeneous catalyst undermicrowave irradiation and solvent- free condition. Optimization of the reaction condition was studiedby the response surface method (Box Behnken Design (BBD)) with three replicates at a central point fordeveloping a second order model. Predicting response values using the obtained model were in a goodaccordance with the experimental results. Clean reaction, easy workup procedure, the reusability of thecatalyst, short reaction times and high yields were some advantages of this work.
پژوهشگران محمدعلی زلفی گل (نفر اول)، اردشیر خزایی (نفر دوم)، نگین سرمستی (نفر سوم)، جابر یوسفی سیف (نفر چهارم)، وحید خاکی زاده (نفر پنجم)، احمد رضا موسوی زارع (نفر ششم به بعد)