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Title FDU-12@AGA-Pd: A novel, green, recyclable, and highly versatile catalyst for C­ C bond formation and synthesis of lH-tetrazoles derivatives
Type Presentation
Keywords 1H-Tetrazo1e; FDU-12, Green, Nano, Catalyst.
Abstract In this work, a novel and efficient nanocatalyst through the immobilization of AGA-Pd e inside of mesoporous silica FDU-12 channels was successfully synthesized by a procedure. The catalytic activity of the described catalyst was investigated for the sis of the Suzuki reaction and lH-tetrazole derivatives. Inthis research, the catalyst was d by the immobilization of Palladium on ordered mesoporous silica (FDU-12) coated Amino-5-guanidinovaleric acid (AGA). N2 adsorption-desorption isotherms indicated nt BET surface area for FDU-12 and FDU-12@AGA-Pd is 627.27 and 106.69 (m2 /g) ively. The physical and chemical properties of raw and modified samples (FDU-12, 2@AGA-Pd) were characterized by TGA, EDX, BET, XRD, ICP, Map, and Fourier­ rm infrared spectroscopy (FT-IR) analyses. This designed nanocatalyst offers several ages including the use of inexpensive materials and commercially available, high yield, eaction times, and simple procedure. The synthesized mesoporous nanocatalyst was red and reused in five continuous cycles without considerable change in its catalytic
Researchers Arash Ghorbani-Choghamarani (Second Researcher), Hamid Aghavandi (First Researcher)