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Title Design and preparation of [4,40-bipyridine]-1,10- diium trinitromethanide (BPDTNM) as a novel nanosized ionic liquid catalyst: application to the synthesis of 1-(benzoimidazolylamino)methyl-2- naphthols†
Type JournalPaper
Keywords [4,40-bipyridine]-1,10- diium trinitromethanide 1-(benzoimidazolylamino)methyl-2- naphthols
Abstract In this work, the novel bifunctional nanosized ionic liquid catalyst [4,40-bipyridine]-1,10-diium trinitromethanide (BPDTNM) was designed, synthesized, and characterized by using FT-IR spectra, 1H and 13C NMR spectra, X-ray diffraction patterns (XRD), scanning electron microscopy (SEM), high resolution transmission electron microscopy (HRTEM), thermogravimetry (TG), derivative thermogravimetry (DTG) analysis, differential thermal analysis (DTA), and HPLC-mass spectroscopy. The synthesized nanosized catalyst was successfully applied to the synthesis of 1-(benzoimidazolylamino)methyl-2-naphthol derivatives via a straightforward one-pot three-component condensation reaction of 2-aminobenzimidazole, 2-naphthol, and a wide range of aromatic aldehydes under mild and solvent-free conditions.
Researchers Asiye Asgari (Not In First Six Researchers), Yadollah Bayat (Not In First Six Researchers), Mehdi Kalhor (Not In First Six Researchers), Abbas Khoshnood (Fifth Researcher), Diego Alonso (Fourth Researcher), (Third Researcher), ma z (Second Researcher), Meysam Yarie (First Researcher)