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Title Perchloric Acid-Functionalized Silica Nanosphere as Novel and Green Catalyst for the Synthesis of 2H-indazolo[2,1-b]phthalazinetrione Derivatives
Type JournalPaper
Keywords Silica nanosphere, silica perchloric acid nanosphere, dimedone, 2H-indazolo[2,1-b]phthalazinetrione derivatives, solvent-free.
Abstract In this report, synthesis and characterization of silica perchloric acid nanosphere as a novel and heterogeneous catalyst are described. It has a spherical shape and the particle size is between 75 and 100 nm. The catalytic activity has been investigated in coupling reaction involving a variety of aldehydes, phthalhydrazide, dimedone at 80°C under solvent-free conditions. This method offers advantages such as good yields, simple conditions, shorter reaction time, and reusable activity catalyst
Researchers Mohammad Hossein Fekri (Fourth Researcher), sadegh rahmati (Third Researcher), Ardeshir Khazaei (Second Researcher), mahdieh chegeni (First Researcher)