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Title
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Synthesis and characterisation of b-tricalcium phosphate coating on zirconia toughened alumina by biomimetic method
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Type
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JournalPaper
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Keywords
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Calcium deficient hydroxyapatite, Biomimetic, b-TCP, Growth, Nucleation, Sodium silicate, Zirconia toughened alumina
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Abstract
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The present work studied bioactive coatings on the surface of ceramic biomaterials. Zirconia toughened alumina (ZTA) composites containing 15 mol.-%. Partially stabilised zirconia was prepared after 1 h sintering at 1550uC. Apatite layers were then coated onto the surfaces of composites by the biomimetic method using 1?5–2 multiply concentrations of simulated body fluid (SBF). Before treatment in SBFs, a sodium silicate layer was employed as nucleating agent to induce the formation of a calcium phosphate layer. The effect of immersion time on the morphology of the precipitate was monitored with a scanning electron microscope. X dot maps revealed that there is a relationship between distribution of Ca–P and ZTA surface. X-ray diffractometry patterns, calcium/phosphor molar ratio and Fourier transform infrared spectroscopy showed that b-tricalcium phosphate and calcium deficient hydroxyapatite precipitated onto substrates via biomimetic. The thin filmX-ray diffraction pattern showed that the calciumdeficient hydroxyapatite decomposed into b-tricalcium phosphate and CaO after 0?5 h of heat treatment at 700uC.
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Researchers
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smaeil salahi (Third Researcher), Ali Nemati (Second Researcher), Hamid Esfahani (First Researcher)
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