In the recent few years, polymer based nanomaterials are emerged as promising candidates in new generation catalysis. In this regard, we report the synthesis of nickel nanoparticles at mild conditions using porous triazine-thiourea-sulfonamide support (TTSA). The novel heterogeneous polymer support was synthesized by silica template method. The synthetically modified porous material (TTSA@Ni NPs) was analyzed in details over a number of physicochemical methods like, FT-IR, FE-SEM, HR-TEM, EDX, XRD, TGA and ICP-OES. In catalytic exploration we aimed the synthesis of alochohols from the reduction of aldehydes/ketones in water. Furthermore, the prepared green heterogeneous catalyst can be recycled and recovered six times without significant loss in the catalytic activity
